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pressure filter test

pressure filter test

pressure filter test

Product catalog summary
Introduction
The document discusses the history and methodology of the Pressure Filter Test, a standardized method developed for assessing the pressure filter value during the production of masterbatches and compounds. This test is crucial for determining the suitability of pigments in plastic coloring.

Historical Background
In 1998, the CEN Committee Pressure Filter Test was established by several companies, including BASF and Dr. COLLIN GmbH, to create a standardized method for determining pressure filter values. The EN 13900-5 standard was introduced in 2004, providing a unique measuring method for pigment suitability in plastics.

Test Methodology
The Pressure Filter Test involves melting and homogenizing the material in an extruder, then passing it through a screen with a constant volume flow. The test measures the pressure increase caused by particles clogging the screen. The lower the pressure, the better the pigment dispersion and product quality.

Advantages
  • Quick filter changes with a cassette system.
  • Bypass valve allows melt flow interruption without stopping the extruder.
  • Integrated pre-heating of the screen.
  • User-friendly software for calculating pressure filter values.


Technical Specifications
According to ISO 23900-5, the test requires specific equipment and conditions, such as a screw diameter of 19-30 mm, a melt pump, and a defined throughput. The standard operating temperature is 300°C, with a high-temperature version available.

Test Procedure
  1. Mount the screen-pack.
  2. Start the test line with basic polymer.
  3. Load test mixture in the hopper.
  4. Begin the test.
  5. Purge with 100 g basic polymer.
  6. Stop the test.
  7. Purge again with 100 g basic polymer.


Test Results
The filter value (FPV) is calculated using the formula: FPV = (P max – P Start) / W, where P max is the maximum pressure, P Start is the initial pressure, and W is the initial pigment weight. An end filter value (FPV end) is also calculated.

Automated Pressure Filter Test
The automated version allows for fully-automatic, standardized quality control of polymers, with automatic screen changes and direct application in production extruders.

Conclusion
The Pressure Filter Test is a critical tool for ensuring the quality of pigments in plastic production, offering standardized procedures and automated options for efficient quality control.
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Catalog excerpts

pressure filter test-1

PRESSURE FILTER TEST The real history behind the Pressure Filter Test More than 25 years successful in the determination of the pressure filter value during the production of masterbatches and compounds

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pressure filter test-2

PRESSURE FILTER TEST The real history behind the Pressure Filter Test More than 25 years successful in the measuring of the pressure filter value during the production of masterbatches and compounds In 1998, several companies founded the „CEN Committee Filtertest“ (CEN Committee Pressure Filter Test): BASF, Clariant, Degussa, Ciba, GABRIEL-CHEMIE as well as Dr. COLLIN GmbH, Brabender Messtechnik and Thermo Electron – manufacturers of laboratory lines for the plastic processing industry. This initiative had the aim to develop a standardized method for the determination of the pressure filter value...

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pressure filter test-3

Extra options pressure filter test at the test extruder ► Fortesting larger quantities of polymer, which require higher throughputs, the measuring head is mounted on an extruder with a screw diameter of 25 mm or 30 mm. ► The filter test is mounted on a movable unit, that increases ► A PC, connected with the line, measures the melt pressure in front of the filter, the melt temperature and the melt pump speed. Pigments and Extenders - Methods of dispersion and / or assessment of dispersibility in plastics - Part 5: What does the norm say Screw diameter Melt pump Test amount Theoretical throughput...

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pressure filter test-4

ISO 23900-5 – Test Procedure 1. Mount the screen-pack 2. Start the test line with basic test polymer 3. Load test mixture in hopper 4. Start of the test 5. Purge with 100 g basic test polymer 6. Stop of the test 7. Purge with 100 g basic test polymer ISO 23900-5 – Test Result Evaluation and visulalisation of the measurement = filter value, bar/g = maximum pressure, bar = initial pressure, bar = initial pigment weight, g Curve depends on test material Possible pressure drop because of rheological characteristics This calculation refers to the standard EN13900-5 resp. ISO 23900-5. Purging with...

 Open the catalog to page 4

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