PAL Smart SPME Fibers
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Ingenious sample handling PAL Smart SPME Fibers Optimized for Automation

PAL3 Smart SPME Fibers Excellent extraction properties combined with smart handling and operational safety Full traceability • Each SPME Fiber is equipped with its unique Smart chip containing parameters, ranges and usage history. • Automatic application of the correct parameters for the individual Smart SPME Fibers. • Color coded for easy identification of coating type and thickness.

PAL3 Smart SPME Fiber Since its introduction by Pawliszyn et al. (ref. 1) Solid Phase Micro Extraction (SPME) has seen a tremendous development. SPME is a very effective way of automated sample preparation. It is used for extracting organics from a matrix (solid, liquid or gaseous) into a stationary phase immobilized on a fiber. The analytes are thermally desorbed directly in the injector of a gas chromatograph. PAL SPME Fibers have been developed and optimized for the most successful SPME sampler, the PAL System Autosampler. The fibers are offered with different coatings and film...

Comparison of PAL Smart SPME Fibers with established Fibers The new PAL SPME Fibers (PDMS fibers 7 μm, 30 μm, and 100 μm and the polyacrylate fiber) yield identical results when compared with the corresponding commercial fibers. For medium and high boiling compounds the PAL SPME Carbon WR Fiber in certain cases shows an even better performance than the established fibers. 1 1,1-Dichloroethene 2 cis-1,2-Dichloroethene 3 Benzene 4 Trichloroethylene 5 Toluene 6 Ethylbenzene 7 m-,p- Xylene 8 o-Xylene 9 Bromobenzene 10 2-Chlorotoluene 11 1,3,5-Trimethylbenzene 12 4 Chlorotoluene 13...

85 jm Acrylate 30 jm PDMS 7 jm PDMS 600 Molecular Weight of Analyte Fig. 2: Correlation between molecular weight of the analyte and the fiber type Table 3: Which fiber for which type of analyte?

The PAL Smart SPME Fibers are available in order quantities of one, three or five fibers per box. For method development, a set of each fiber type (set of five) is available. No. Stationary Color Set of 1 Smart Fiber Set of 3 Smart Fibers Set of 5 Smart Fibers Phase Code Description PNo. Description PNo. Description PNo. PDMS Smart SPME Fiber (Polydimethylsiloxane) DVB /PDMS/ Carbon WR Smart SPME Fiber (Divinylbenzene / Polydimethylsiloxane / Carbon Wide Range) 7 80 pm (50 pm / 30 pm) Black SFIB-DVB/C-WR-80/10-P1 SFIB-DVB/C-WR-80/10-P3 SFIB-DVB/C-WR-80/10-P5 Smart Fiber Selections for...

PAL RTC / PAL RSI The robotic tool change exclusively available with the PAL RTC allows for the automatic exchange of fibers, e.g. for the automated development of SPME methods. Smart SPME Kit PNo.: PAL3-SPME-SFib-Kit SPME Arrow Conditioning Module PNo.: PAL3-SPME-ArrowCond Kit containing – SPME Tool – Smart SPME Fiber Collection (one of each type) – SPME Performance Evaluation Mix – For the conditioning of Smart SPME fibers and Smart SPME Arrows prior to sample collection – Temperature range up to 350°C – Purge gas connection for more efficiency The Agitator Module provides 6 positions for...

For more information on the PAL System visit: www.palsystem.com 0SI0si PAL is a registered trademark of CTC Analytics AG, Switzerland