MFS-2015E

MFS-2015E

MFS-2015E

Product catalog summary
System Configuration
The Multi-Functional Splitless Sampler (MFS) is composed of three main units: a pre-column, a splitter, and an MFS Flow Controller. The pre-column is connected between the gas chromatograph (GC) inlet and the separation column. The MFS Flow Controller, which includes a suction pump and a flow regulator, can be programmed via software included with Frontier Lab’s pyrolyzer package.
Specifications
  • New Splitless Pyrolysis: Enables high-sensitivity detection of trace pyrolyzates and solvent venting.
  • Backflush: Reduces analysis time by preventing high-boiling compounds from entering the separation column.
  • Peak Separation Improvement: Enhanced peak separation through the selection of an appropriate pre-column.
Supported Columns
The system supports deactivated metal columns (Ultra ALLOY®) and FS capillary columns with internal diameters of 0.25 and 0.32 mm.
Required Equipment
  • Compatible GC or GC/MS models include Agilent 5977, 5975, 8890, and 7890 GC; JEOL JMS-Q1500GC; Shimadzu QP2020 NX, GC-2030; Thermo Fisher ISQ series, TRACE1600 series, 1300 series.
  • Requires the ability to close the split vent and septum purge simultaneously for Splitless Pyrolysis.
  • Required pyrolyzer: Multi-Shot Pyrolyzer (EGA/PY-3030D).
  • Analysis method: Flash pyrolysis (Single-shot analysis) only.
Compatible Accessories
  • Auto-Shot Sampler (AS-1020E)
  • MicroJet Cryo-Trap (MJT-1030Ex, MJT-1035E, MJT-2030E)
Power Requirement
100 ~ 240 VAC, 40 VA
Key Features of MFS
  • New Splitless Pyrolysis: Increases sensitivity by about 50 times compared to the split pyrolysis method by using a higher helium flow rate (15 mL/min).
  • Solvent Venting: Unwanted components such as solvents are vented from the system before entering the separation column.
  • Backflushing: Prevents contamination and shortens analysis time by removing high-boiling compounds from the pre-column.
  • Peak Separation Improvement: Achieved by selecting a pre-column with a different polarity and optimal length.
Patent Information
Japanese Patent 7142374
Conclusion
The MFS is a specialized accessory for the Multi-Shot Pyrolyzer, offering advanced features like New Splitless Pyrolysis, backflush, and improved peak separation, enhancing the efficiency and accuracy of pyrolysis analysis.
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Catalog excerpts

MFS-2015E-1

Featured by New Splitless Pyrolysis, Backflush, and Improved separation Multi-Functional Splitless Sampler MFS-2015E Japanese Patent 7142374 This product is a peripheral accessory exclusively used with the Multi-Shot Pyrolyzer (EGA/PY-3030D), which allows for the new Splitless Pyrolysis, backflush, solvent cut, and improves peak separation. Features of MFS 1. New Splitless Pyrolysis: High-sensitivity detection of trace pyrolyzates and solvent venting 2. Backflush: Shortens analysis time by blocking high-boiling compounds from flowing into separation column 3. Peak separation improvement: Improved peak separation by selecting an appropriate pre-column System configuration 3) MFS Flow Controller Pyrolyzer Flow regulator Temperature Controller The MFS consists of three units: (1) a precolumn connected between the GC inlet and a separation column, (2) a splitter between the pre-column and the separation column, and (3) MFS Flow Controller consisting of a suction pump and a flow regulator. The operation of MFS Flow Controller can be programmed through the software that comes standard in the Frontier Lab’s pyrolyzer package. Separation Column Control Software Specifications Supported columns Deactivated metal column (Ultra ALLOY®) and FS capillary column, i.d. 0.25 and 0.32 mm Agilent JEOL Required GC or GC/MS (alphabetical order) Thermo Fisher ISQ series, TRACE1600 series, 1300 series Each of the above instrument requires the ability to close the split vent and septum purge at the same time for Splitless Pyrolysis. Please contact us for more information. Required pyrolyzer* Multi-Shot Pyrolyzer (EGA/PY-3030D) only Analysis method Flash pyrolysis (Single-shot analysis) only Compatible accessory Auto-Shot Sampler (AS-1020E) MicroJet Cryo-Trap (MJT-1030Ex, MJT-1035E, MJT-2030E) Power requirement

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MFS-2015E-2

Three Features of MFS In the analysis examples below, the following columns are used. • Pre-column: Ultra ALLOY+-50 (50 % diphenyl 50 % dimethylpolysiloxane), L=2 m, i.d. 0.25 mm df. 1.0 µm • Separation column : Ultra ALLOY+-5 (5 % diphenyl 95 % dimethylpolysiloxane), L=30 m, i.d. 0.25 mm, df. 0.5 µm 2. Shortened analysis time by backflushing (BF) 1.1 High-sensitivity detection of trace pyrolyzates In normal splitless pyrolysis, the He flow rate is as low as 4 mL/min, causing secondary reactions that greatly change the pyrogram profile. 15 mL/min of He flow rate with the MFS suppresses secondary...

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