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XRD-6100

XRD-6100
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XRD-6100

Product catalog summary
Overview: The document provides comprehensive information on the XRD-6100 X-ray Diffractometer by Shimadzu Corporation, detailing its features, applications, and technical specifications. It is intended for research purposes and not for diagnostic use.
Key Features:
  • Ease of Use: Equipped with a vertical goniometer and Windows-supported software, the XRD-6100 is user-friendly and suitable for diverse analyses.
  • High Precision: The compact goniometer is pre-adjusted for accuracy, requiring no user adjustments.
  • Software Platform: Utilizes Windows 10 for data processing and network support, facilitating easy data export and multi-user access.
  • Auto-Search/Match Software: Includes qualitative and quantitative analysis software with detailed search parameters and the RIR method for simplified calculations.
  • Compact Design: Energy-efficient with safety features like an X-ray off mechanism when the door is open.
  • High-Speed Detector: The OneSight detector enhances analysis capabilities with high intensity.
Applications:
  • Metals: Analyzes residual stress, texture, and surface conditions in metals like steel and aluminum.
  • Chemicals and Catalysts: Conducts qualitative analysis and crystallite size measurement of organic/inorganic chemicals and catalysts.
  • Ceramics and Glass: Analyzes raw materials, final products, and thin film layers.
  • Pharmaceuticals: Evaluates raw materials, impurities, and crystal polymorphism for quality control.
  • Resources and Energy: Assesses impurities and asbestos content in coal, oil, natural gas, and minerals.
  • Electrical and Electronic Materials: Analyzes corrosion, stress, and crystal orientation in electronic components.
  • Environment and Industrial Wastes: Analyzes asbestos, silicic acids, and residual matter in industrial waste.
Principle of the Polycapillary Optical System: Utilizes fine glass capillaries to guide X-rays through total internal reflection, resulting in a parallel beam with a large solid angle, providing higher diffraction X-ray intensity and accurate measurements even with sample displacement or irregular surfaces.
Sample Measurement Using the Polycapillary Optical System: Used for measuring raw acetaminophen and its tablets, evaluating crystallinity and polymorphism with accuracy on irregular or curved surfaces.
Qualitative and Quantitative Analysis of Asbestos and Free Silicic Acids: Involves pulverizing samples, qualitative analysis, and quantitative analysis using X-ray diffractometry, requiring high sensitivity to detect trace asbestos levels.
XRD-6100 X-ray Diffractometer: Supports various X-ray tubes and provides stable operation with high precision, used for analyzing crystalline states and offering non-destructive testing under normal atmospheric conditions.
Specifications and Features: Allows for detailed search parameters and the creation of dedicated user databases, supporting qualitative and quantitative analysis, peak processing, and crystallinity calculations.
Database and Search Functions: Utilizes PDF-2 or PDF-4 databases for detailed data display, featuring a second search function for identifying small amounts of components.
Calibration and Quantitative Analysis: Calibration curves can be created using three methods: external standard, internal standard, and standard addition, with software supporting intensity and integrated intensity modes.
OneSight Wide-Range High-Speed Detector: Increases measurement speed and sensitivity, offering three measurement modes and allowing for simultaneous diffraction profile measurement over a wide angle.
Environmental Analysis: Addresses environmental analysis challenges with software that corrects for X-ray absorption by filters, providing accurate calibration curves.
Specifications: Features a scintillator Na I and a scaler with a preset time ranging from 0.1 to 1000 seconds, supporting various X-ray tubes with power ratings from 1.0kW to 2.7kW.
Installation Requirements: Compliance with local X-ray regulations is necessary, with specific temperature, humidity, and power requirements for installation.
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Catalog excerpts

XRD-6100-1

X-ray Diffractometer

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XRD-6100-2

Ease of Use and Abundant Functions Herald a New Era of Analysis The Windows-supported application software ushers this compact, multi-functional, general-purpose X-ray Diffractometer into the networking era of analysis. X-Ray Diffractometer In addition to its basic ease of use and abundant functions, the XRD-6100 boasts an integrated design featuring a vertical goniometer and data processing software supporting the Windows user interface. The XRD-6100 offers solutions encompassing wide-ranging analysis requirements, from routine qualitative and quantitative analysis to state change analysis,...

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XRD-6100-3

A General-Purpose X-ray Diffractometer to Address Your Various Analytical Needs Fe a tu res Hi g h -Prec i s i o n a nd Re lia ble Built -in Ve r t ica l G oniom e t e r The goniometer mounted on the XRD-6100 is compact and simple. All the components in the X-ray optical system are precisely assembled and adjusted at the factory and have been designed to ensure that accuracy is maintained. Thus, there is absolutely no need for users to make any adjustments in the future. Wi n d o ws 10 Em ploy e d a s S of t w a re P la t f or m The main unit control and data processing software support the widely...

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XRD-6100-4

Applications of X-ray Diffractometry F e rro u s Meta ls Steel Qualitative analysis of steel sheet, measurement of residual austenite and residual stress, analysis of friction and wear test samples, measurement of iron oxide films and nitride layers, evaluation of plating and texture. Cast Iron Qualitative analysis of precipitates and additives in cast iron, etc. Surface-Treated Steel Evaluation of characteristics of surface-treated areas, quality control, residual stress measurement. N o n - F e rro u s Meta ls Copper and Zinc Qualitative analysis of alloys, orientation measurements of foil...

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XRD-6100-5

Pharmac eutic als and M edic al Treat m en t Pharmaceuticals Qualitative analysis of pharmaceutical raw materials and identification of impurities. Crystal polymorphism analysis and crystallinity measurements, quality control during pharmaceutical manufacture using crystallite size measurement, final product quality check, crystal polymorphism analysis related to patents. Dental Materials Qualitative analysis of dental materials such as apatite, etc. Electrical and Electronic Materials Electrical Components Qualitative analysis of corrosion and adhering matter on electrical contacts. Stress measurements...

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XRD-6100-6

Polycapillary Optical System Principle of the Polycapillary Optical System Schematic Diagram of the Polycapillary Optical System The fine glass capillaries in the order of several microns are arranged in a solid as guides to multiple X-rays. The X-rays pass along each capillary while repeating total internal reflection and exit from the opposite end of the polycapillary system. The capillaries are curved so that repeated total internal reflection is allowed, and the X-rays from the point X-ray source exit the unit as a parallel beam with a large solid angle. Output divergence angle 0.22° Intake...

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XRD-6100-7

Qualitative and Quantitative Analysis of Asbestos and Free Silicic Acids The content of asbestos in construction materials is measured using phase dispersion microscopes and X-ray diffractometers. After pulverizing the sample acquired from the site in a pulverizer, a phase dispersion microscope and X-ray diffractometer are used respectively to qualitatively analyze the sample. If the sample is determined to contain asbestos at this stage, then it is quantitatively analyzed using the X-ray diffractometer. In actual practice, asbestos analysis (JIS A 1481-3) requires sensitivity sufficient to determine...

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XRD-6100-8

Cons truc tion The XRD-6100 analyzes crystalline states under normal atmospheric conditions. Furthermore, this method is non-destructive. X-rays hit a sample loaded in the center of the goniometer and are diffracted by the sample. The changes in the diffracted X-ray intensities are measured, recorded and plotted against the rotation angles of the sample. The result is referred to as the X-ray diffraction pattern of the sample. Computer analysis of the peak positions and intensities associated with this pattern enables qualitative analysis, lattice constant determination and/or stress determination....

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XRD-6100-9

X-ray Tubes Highly Stable X-ray Generator The XRD-6100 will accept various types of X-ray tubes, including the normal focus (NF) 2kW type and broad focus (BF) 2.7kW type, which are standard accessories, as well as the optional long fine focus (LFF) 2.2kW type. By attaching the optional counter monochromator, all types of samples, including Fe samples, can be analyzed using the standard Cu X-ray tube. Shimadzu's extensive experience in producing high-performance X-ray generators has enabled the production of a highly stable X-ray generator, with tube voltage and tube current both stable to within...

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XRD-6100-10

Providing a Complete Analysis System Analysis System Standard Software X-ray generator control Optical path adjustment X-ray ON/OFF, tube voltage/current setting Goniometer adjustment Detector adjustment Single scan, multi-scan File maintenance ASCII data conversion ASCII data to XRD-6100 data conversion XD-D1 data to XRD-6100 data conversion Basic data processing Graphic display Smoothing, background elimination, Kα1-Kα2 separation, peak search, system error correction, internal/external standard correction, operations between data Vertical display, horizontal display Overlay display (3D) Log...

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XRD-6100-11

Automatic Measurement, Easy Operation Measurement Display Sample measurement conditions can be set easily. The scheduling and the progress condition of the measurement can be confirmed in one view by the analysis & spooler. Measurement Screen Multitasking for Enhanced Analysis Efficiency Basic Data Processing The multitasking capability provided with the Windows operating environment allows measurement and data processing to be conducted simultaneously, enhancing the efficiency of analysis operations. Basic Data Processing Screen

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